HIGH RESOLUTION NMR IN SOLIDS SELECTIVE AVERAGING SUPPLEMENT 1 ADVANCES IN MAGNETIC RESONANCE

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High Resolution Nmr In Solids Selective Averaging

Author : Ulrich Haeberlen
ISBN : 9780323160254
Genre : Science
File Size : 24.1 MB
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High Resolution NMR in Solids: Selective Averaging presents the principles and applications of the four approaches to high resolution NMR in solids — magic-angle sample spinning, multiple-pulse, proton-enhanced nuclear induction, and indirect detection methods. Divided into six chapters, this book initially describes the tensorial properties of nuclear spin interactions in both ordinary and spin spaces. It then deals with the manifestations of nuclear magnetic shielding in NMR spectra of both single-crystal and powder samples, and then discusses the techniques for analyzing spectra and rotation patterns in terms of shielding tensors. A wide range of NMR phenomena that are result of intentional or natural, selective or unselective averaging processes and the average Hamiltonian theory that yields the inclusion of correction are covered. This book also provides a detailed discussion on multiple-pulse sequences intended for high resolution NMR in solids. The concluding chapter examines the applications of multiple-pulse techniques, with particular emphasis on measurements of 19F and 1H shielding tensors. Discussions on rotations of angular momentum operators; time ordering and the Magnus expansion; off-resonance averaging of the second-order dipolar Hamiltonian; and phase transients are covered in the supplemental texts.
Category: Science

Spectroscopic Properties Of Inorganic And Organometallic Compounds

Author : E A V Ebsworth
ISBN : 9781847554949
Genre : Science
File Size : 74.69 MB
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Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr
Category: Science

Pulsed Magnetic Resonance Nmr Esr And Optics

Author : Erwin Louis Hahn
ISBN : 0198539622
Genre : Science
File Size : 28.81 MB
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These articles written as a tribute to E. L. Hahn on his 70th birthday, present a stimulating, and perhaps controversial contribution to the literature, which will be of interest to students and research workers in a wide variety of disciplines.
Category: Science

Advances In Magnetic And Optical Resonance

Author : Warren S. Warren
ISBN : 0080526306
Genre : Science
File Size : 31.44 MB
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Since 1965, Advances in Magnetic and Optical Resonance has provided researchers with timely expositions of fundamental new developments in the theory of, experimentation with, and application of magnetic and optical resonance.
Category: Science

Solid State Nmr Of Polymers

Author : T. Asakura
ISBN : 0080541461
Genre : Science
File Size : 88.68 MB
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In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods. This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described. Features of this book: • Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field • Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists. This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.
Category: Science

Spectroscopic Properties Of Inorganic And Organometallic Compounds

Author :
ISBN : UCAL:B3916046
Genre : Chemistry, Inorganic
File Size : 58.75 MB
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Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr
Category: Chemistry, Inorganic

Fundamentals Of Nuclear Magnetic Resonance

Author : Jacek W. Hennel
ISBN : 0582067030
Genre : Medical
File Size : 31.67 MB
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Simple and precise explanation of the physical and mathematical foundations of nuclear magnetic resonance (NMR).
Category: Medical

Coherence And Nmr

Author : M. Munowitz
ISBN : 0471615234
Genre : Science
File Size : 78.73 MB
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Places into perspective the role of quantum dynamics in NMR--addresses characterization of a system of particles with spin (or any other quantum mechanical property), how such a system changes with time, and broader applications to chemistry, physics, and other fields. Also ties together the various manifestations of NMR in solids and liquids--using as a common language the unitary transformation of a system's density operator under the Hamiltonian--revealing the underpinnings of what might be called manipulative NMR: experiments in which the time-dependent Schdinger equation is controlled externally in a non-trivial fashion.
Category: Science